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Changes in magmatism and sedimentation along the late Neoproterozoic-early Paleozoic Ross orogenic belt in Antarctica have been linked to the cessation of convergence along the Mozambique belt during the assembly of East-West Gondwana. However, these interpretations are non-unique and are based, in part, on limited thermochronological data sets spread out along large sectors of the East Antarctic margin. We report new 40Ar/39Ar hornblende, muscovite, and biotite age data for plutonic (n = 13) and metasedimentary (n = 3) samples from the Shackleton–Liv Glacier sector of the Queen Maud Mountains in Antarctica. Cumulative 40Ar/39Ar age data show polymodal age peaks (510 Ma, 491 Ma, 475 Ma) that lag peaks in U-Pb igneous crystallization ages, suggesting igneous and metamorphic cooling following magmatism within the region. The 40Ar/39Ar ages are similar to ages in other sectors of the Ross orogen, but younger than detrital mineral 40Ar/39Ar cooling ages indicative of older magmatism and cooling of unexposed inboard areas along the margin. Detrital zircon trace element abundances suggest that the widespread onset of magmatism in outboard localities of the orogen correlates with a ~560–530 Ma decrease in crustal thickness. The timing of crustal thinning recorded by zircon in magmas overlaps with other evidence for the timing of crustal extension, suggesting that the regional onset of magmatism with subsequent igneous and metamorphic cooling probably reflects slab rollback that coincided with possible global plate motion changes induced during the final assembly of Gondwana. 

Abstract Orientated carbonate (calcite twinning strains; n = 78 with 2414 twin measurements) and quartzites (finite strains; n = 15) were collected around Gondwana to study the deformational history associated with the amalgamation of the supercontinent. The Buzios orogen (545–500 Ma), within interior Gondwana, records the high-grade collisional orogen between the São Francisco Craton (Brazil) and the Congo–Angola Craton (Angola and Namibia), and twinning strains in calc-silicates record a SE–NW shortening fabric parallel to the thrust transport. Along Gondwana's southern margin, the Saldanian–Ross–Delamerian orogen (590–480 Ma) is marked by a regional unconformity that cuts into deformed Neoproterozoic–Ordovician sedimentary rocks and associated intrusions. Cambrian carbonate is preserved in the central part of the southern Gondwana margin, namely in the Kango Inlier of the Cape Fold Belt and the Ellsworth, Pensacola and Transantarctic mountains. Paleozoic carbonate is not preserved in the Ventana Mountains in Argentina, in the Falkland Islands/Islas Malvinas or in Tasmania. Twinning strains in these Cambrian carbonate strata and synorogenic veins record a complex, overprinted deformation history with no stable foreland strain reference. The Kurgiakh orogen (490 Ma) along Gondwana's northern margin is also defined by a regional Ordovician unconformity throughout the Himalaya; these rocks record a mix of layer-parallel and layer-normal twinning strains with a likely Himalayan (40 Ma) strain overprint and no autochthonous foreland strain site. Conversely, the Gondwanide orogen (250 Ma) along Gondwana's southern margin has three foreland (autochthonous) sites for comparison with 59 allochthonous thrust-belt strain analyses. From west to east, these include: finite strains from Devonian quartzite preserve a layer-parallel shortening (LPS) strain rotated clockwise in the Ventana Mountains of Argentina; frontal (calcite twins) and internal (quartzite strains) samples in the Cape Fold Belt preserve a LPS fabric that is rotated clockwise from the autochthonous north–south horizontal shortening in the foreland strain site; Falkland Devonian quartzite shows the same clockwise rotation of the LPS fabric; and Permian limestone and veins in Tasmania record a thrust transport-parallel LPS fabric. Early amalgamation of Gondwana (Ordovician) is preserved by local layer-parallel and layer-normal strain without evidence of far-field deformation, whereas the Gondwanide orogen (Permian) is dominated by layer-parallel shortening, locally rotated by dextral shear along the margin, that propagated across the supercontinent. 

Orogenic crustal thickening leads to increased continental elevation and runoff into the oceans, but there are fundamental uncertainties in the temporal patterns of thickening through Earth history. U‐Pb age and trace element data in detrital zircons from Antarctica are consistent with recent global analyses suggesting two dominant peaks in average crustal thickness from ~2.6 to 2.0 Ga and ~0.8 to 0.5 Ga. Shifts in marine carbonate 87Sr/86Sr ratios show two primary peaks that post‐date these crustal thickness peaks, suggesting significant weathering and erosion of global continental relief. Both episodes correlate well with zircon trace element and isotope proxies indicating enhanced crustal and fluid input into subduction zone magmas. Increased crustal thickness correlates with increased passive margin abundance and overlaps with snowball Earth glaciations and atmospheric oxygenation, suggesting a causal link between continental rift‐drift phases and major transitions in Earth's atmospheric and oceanic evolution. 

The Ross orogenic belt in Antarctica is one of several Neoproterozoic-early Palaeozoic orogens that crisscrossed Gondwana and are associated with Gondwana’s assembly. We present new age data from the Queen Maud Mountains, Ross orogen, from areas that hitherto have lacked precise ages from the local plutonic rocks. The zircon U-Pb igneous crystallization ages (n = 7) and a hornblende 40Ar/39Ar cooling age (n = 1) constrain plutonism to primarily lie within the Cambrian to Ordovician. Cumulative zircon U-Pb crystallization age data yield polymodal age distributions (516 Ma, 506–502 Ma, and 488 Ma age peaks) that are similar to other areas of the Queen Maud-Horlick Mountains, consistent with regional magmatic flare-ups along the Pacific-Gondwana margin during these times. The ages of deformed plutons constrain deformation to the Cambrian (Series 2) to Ordovician (Lower), with some regions indicating a transition to post-tectonic magmatism and cooling at ~509-470 Ma. Collectively, the data indicate that the Queen Maud-Horlick Mountains share a similar petrotectonic history with other regions of the Pacific-Gondwana margin, providing new evidence that this tectonostratigraphic province is part of and not exotic to the larger igneous-sedimentary successions developed in the peri-Gondwana realm under a broadly convergent margin setting.